Your current setup file is: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302.par
 
Goniometer type: KM4 (km4gonio.xdll)
Your current setup file is: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302.par

WINDOWS INFORMATION: (44.70a 64-bit (release 10-09-2024))
System version: WINDOWS 10, Build: 19045
Screen resolution:2560x1440 (Primary screen); Fonts: 96; Color: 32 bits; monitors: 2

HYPIX CAMERA INTERFACE
Reading tabbin file: "D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_peakhunt"
   UB - matrix:
       0.000895    0.004131   -0.001111   (  0.000060    0.000066    0.000014 )
      -0.002027   -0.003252   -0.001772   (  0.000072    0.000080    0.000017 )
      -0.005810   -0.000216   -0.000094   (  0.000115    0.000129    0.000027 )
   M - matrix:
       0.000039    0.000012    0.000003   (  0.000001    0.000001    0.000000 )
       0.000012    0.000028    0.000001   (  0.000001    0.000001    0.000000 )
       0.000003    0.000001    0.000004   (  0.000000    0.000000    0.000000 )
UB fit with 61 obs out of 807 (total:807,skipped:0) (7.56%)
    unit cell:
       4.42(10)   5.10(6)  12.36(14)       
      91.5(10)  103(1)    110(2)     
      V = 254(7) 
Multi-core copying folder files started

================================== COPY FOLDER FILES SUMMARY ===================================
Source folder path: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\csdsearches_online_Rigaku
Target folder path: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\csdsearches_Rigaku
Files copied:
	-5 folder and subfolder(s) file(s)
=============================================================================================

Multi-core copying folder files finished
Shutterless mode turned OFF for pixel detector!!! Switching to ON.
MICROED/3DED INFO: no microED-frames-digest in experiment present!
iIsMicroEDDigestValidMk1MICROEDLIC (rpputils_pro.dll): digest missing, but license ok!
MICROED/3DED INFO: Trying to add digest for future use...
MICROED/3DED INFO: Digest generator ver3 with buffer
MICROEDUTIL_CAP: MicroED license key expires in 2841 days (Wed Jun 30 14:04:46 2032)!
MICROED/3DED INFO: Data set successfully validated for the use with microED-frames-digest (Thu Sep 19 14:04:46 2024)
MICROED/3DED INFO: microED-frames-digest is valid (license:1)!
MICROEDUTIL_CAP: MicroED license key expires in 2841 days (Wed Jun 30 14:04:46 2032)!
PROFFITIO INFO: Creating PROFFIT lock file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302.proffitlock
DC PROFFIT INFO: Concurrent data reduction resumed offline

Process information (Thu Sep 19 14:04:47 2024)
ID: 20788; threads 37; handles 1189; mem 381056.00 (5358528.00)kB; time: 2s

MEMORY INFO: Memory PF:12932.0, Ph:7803.0, V:5231.0;  
MEMORY INFO: Process info - Handles: 1187, Memory: PF:372.3,peak PF: 401.3, WS: 299.4, peak WS: 329.0
MEMORY INFO: RED G:4.6,H:0.5 (#993),V:158.7 (#25)
MEMORY INFO: Tracker: RED 161.5 (#6)
MEMORY INFO: Image pool: RED 6.8/100.0 (#6, page size: 4096)
MEMORY INFO: tracker memory not in use!
MEMORY INFO: tracker memory not in use!
MEMORY INFO: tracker memory not in use!
 
MEMORY INFO: Memory PF:12935.0, Ph:7804.0, V:5233.0;  
MEMORY INFO: Process info - Handles: 1187, Memory: PF:374.1,peak PF: 401.3, WS: 301.2, peak WS: 329.0
MEMORY INFO: RED G:4.6,H:0.5 (#993),V:160.5 (#26)
MEMORY INFO: Tracker: RED 163.3 (#7)
MEMORY INFO: Image pool: RED 6.8/100.0 (#6, page size: 4096)
MEMORY INFO: tracker memory not in use!
MEMORY INFO: tracker memory not in use!
MEMORY INFO: tracker memory not in use!
 
DC PROFFIT - Profile-fitting data reduction algorithm (44.70a 64-bit (release 10-09-2024),compiled Sep 10 2024,13:29:26)
DC PROFFIT - Started at Thu Sep 19 14:04:47 2024
Experiment file name: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302
Output file name: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto
Data reduction with automatic settings
   UB - matrix:
       0.000896    0.003948   -0.001096   (  0.000000    0.000000    0.000000 )
      -0.002065   -0.003142   -0.001817   (  0.000000    0.000000    0.000000 )
      -0.005910   -0.000145   -0.000156   (  0.000000    0.000000    0.000000 )
      4.35598 (    0.00000 )     5.29324 (    0.00000 )    12.28017 (    0.00000 )
     92.36692 (    0.00000 )   104.26093 (    0.00000 )   108.65796 (    0.00000 )
  V =       257.77
Selected cell (from UM rr/UM ttt/UM f):
31     4.3560     5.2932    12.2802    92.3669   104.2609   108.6580         aP
Cross checking gral lattice...
Lattice type P selected
AC6 unit cell: 4.35598 5.29324 12.28017 92.36692 104.26093 108.65796
Background parameters (old style):       50       50 SHORT follow:0
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_bg.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_ppcriterion1.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_ppcriterion2.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_predictaccuracyvsframe.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_predictaccuracyvstheta.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_profiles.dat)
DELETE INFO: Deleting dat files... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_profilecorr*.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_latticeperrun.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_refinedsubmodels.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_lattice.dat)
DELETE INFO: Deleting ini file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\expinfo\exp_7302_auto_coverage.ini)
DELETE INFO: Deleting ini file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\expinfo\exp_7302_auto_crystal.ini)
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DELETE INFO: Deleting ini file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\expinfo\exp_7302_auto_datared.ini_report)
DELETE INFO: Deleting rrprof file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.rrpprof)
DELETE INFO: Deleting skipregion txt files... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto_skipregion.txt)
DELETE INFO: Deleting overflow txt files... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto_overflow.txt)
DELETE INFO: Deleting edgeskip txt files... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto_edgeskip.txt)
DELETE INFO: Deleting cif file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.cif)
DELETE INFO: Deleting cif_od file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.cif_od)
DELETE INFO: Deleting _dyn.cif_cap file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto_dyn.cif_cap)
DELETE INFO: Deleting cif_pets file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.cif_pets)
DELETE INFO: Deleting _dyn.cif_pets file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto_dyn.cif_pets)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_absscale.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_absscaleint.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_absscaleintcorr.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_absscaleres.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_absscalerescorr.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_bfactor.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_afactor.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_cover.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_hklplot.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_resolutionstats.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_rint.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_chi2bm.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_chi2am.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_stickabsorption.dat)
DELETE INFO: Deleting dat file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\exp_7302_auto_incidence.dat)
DELETE INFO: Deleting grl file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.grl)
DELETE INFO: Deleting ins file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.ins)
DELETE INFO: Deleting eqv file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.eqv)
DELETE INFO: Deleting hkl file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.hkl)
DELETE INFO: Deleting hklgral file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.hklgral)
DELETE INFO: Deleting p4p file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.p4p)
DELETE INFO: Deleting p4pgral file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.p4pgral)
DELETE INFO: Deleting rint file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.rint)
DELETE INFO: Deleting rint_redun file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.rint_redun)
DELETE INFO: Deleting errmod file... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_auto.errmod)
Per-frame model refinement: ON
Instrument model dd at start: 647.00 mm
Polarization value used during processing 0.5000
Single frame average background scaling: OFF
Single wavelength only: ON 
Pixel HKL filter in PROFFITPEAK: ON
2-cycle 3D peak analysis: ON
General average background pars: Re=50, Fr=50
Smart background: ON (window = 1, saving frames = 0, visualize frames = 0)
Background computed as FLOAT type: ON
Use 3D profile fitting: ON
Adjust masks according to prediction uncertainty (for high angle data): OFF
Follow profile size changes with incidence angle: ON
Reject reflections with bad profiles: OFF
Consider reflection spot drift along diffraction vector: OFF
Overflow threshold: 258122 
Overflow marker: -9999999 
User limits in use: max: 1000.0000 min: 0.8000  
Not used frames (Frames selector): 0 
Use JETSHADOW for masking shadowed areas: OFF

Camera read noise override for background estimation in use: RMS=  1.0
Space group determination with Gral
AutoChem attempted
Laue symmetry par settings: 1 (Friedel:1)
  0 Extinction conditions:

PROFFITPEAK - Precise peak table update based on 3D profile analysis (2005-2024)
PROFFITPEAK - Started at Thu Sep 19 14:04:48 2024
Experiment file name: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302
Maximum reflection width (in deg): 0.50
I/sigma threshold: 7.00

   UB - matrix:
       0.000896    0.003948   -0.001096   (  0.000000    0.000000    0.000000 )
      -0.002065   -0.003142   -0.001817   (  0.000000    0.000000    0.000000 )
      -0.005910   -0.000145   -0.000156   (  0.000000    0.000000    0.000000 )
   M - matrix:
       0.000040    0.000011    0.000004   (  0.000000    0.000000    0.000000 )
       0.000011    0.000025    0.000001   (  0.000000    0.000000    0.000000 )
       0.000004    0.000001    0.000005   (  0.000000    0.000000    0.000000 )
    unit cell:
       4.3560     5.2932    12.2802         
      92.3669   104.2609   108.6580   
      V = 257.7655   
Lattice type P used

*** 3D peak analysis started - run 1 ***
BACKGROUND INFO: Ranges
  - Red run list: start=1, end=496, width=0.250
  - Required frames: #=50, start=1, end=50,
BACKGROUND INFO: Using background file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_1.img
BACKGROUND INFO: Using background sigma file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_backsig_1_1.img
BACKGROUND INFO: Using background info file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_1.rpb
BACKGROUND INFO: Ranges
  - Red run list: start=1, end=496, width=0.250
  - Required frames: #=50, start=51, end=100,
BACKGROUND INFO: Using background file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_51.img
BACKGROUND INFO: Using background sigma file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_backsig_1_51.img
BACKGROUND INFO: Using background info file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_51.rpb
BACKGROUND INFO: Ranges
  - Red run list: start=1, end=496, width=0.250
  - Required frames: #=50, start=101, end=150,
BACKGROUND INFO: Using background file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_101.img
BACKGROUND INFO: Using background sigma file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_backsig_1_101.img
BACKGROUND INFO: Using background info file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_101.rpb
BACKGROUND INFO: Ranges
  - Red run list: start=1, end=496, width=0.250
  - Required frames: #=50, start=151, end=200,
BACKGROUND INFO: Using background file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_151.img
BACKGROUND INFO: Using background sigma file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_backsig_1_151.img
BACKGROUND INFO: Using background info file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_151.rpb
BACKGROUND INFO: Ranges
  - Red run list: start=1, end=496, width=0.250
  - Required frames: #=50, start=201, end=250,
BACKGROUND INFO: Using background file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_201.img
BACKGROUND INFO: Using background sigma file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_backsig_1_201.img
BACKGROUND INFO: Using background info file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_201.rpb
BACKGROUND INFO: Ranges
  - Red run list: start=1, end=496, width=0.250
  - Required frames: #=50, start=251, end=300,
BACKGROUND INFO: Using background file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_251.img
BACKGROUND INFO: Using background sigma file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_backsig_1_251.img
BACKGROUND INFO: Using background info file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_251.rpb
BACKGROUND INFO: Ranges
  - Red run list: start=1, end=496, width=0.250
  - Required frames: #=50, start=301, end=350,
BACKGROUND INFO: Using background file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_301.img
BACKGROUND INFO: Using background sigma file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_backsig_1_301.img
BACKGROUND INFO: Using background info file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_301.rpb
BACKGROUND INFO: Ranges
  - Red run list: start=1, end=496, width=0.250
  - Required frames: #=50, start=351, end=400,
BACKGROUND INFO: Using background file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_351.img
BACKGROUND INFO: Using background sigma file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_backsig_1_351.img
BACKGROUND INFO: Using background info file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_351.rpb
BACKGROUND INFO: Ranges
  - Red run list: start=1, end=496, width=0.250
  - Required frames: #=50, start=401, end=450,
BACKGROUND INFO: Creating background file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_401.img
BACKGROUND INFO: Creating background sigma file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_backsig_1_401.img
BACKGROUND INFO: Creating background info file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_401.rpb
BACKGROUND INFO: Ranges
  - Red run list: start=1, end=496, width=0.250
  - Required frames: #=50, start=451, end=500,
  - Adjusted required frames (end): #=50, start=447, end=496,
BACKGROUND INFO: Creating background file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_447.img
BACKGROUND INFO: Creating background sigma file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_backsig_1_447.img
BACKGROUND INFO: Creating background info file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_back_1_447.rpb
PROFFITPEAK info: 3022 peaks in the peak location table
UB fit with 59 obs out of 916 (total:916,skipped:0) (6.44%)
   UB - matrix:
       0.000756    0.004194   -0.001140   (  0.000055    0.000053    0.000013 )
      -0.002027   -0.003303   -0.001772   (  0.000079    0.000076    0.000018 )
      -0.005792   -0.000120   -0.000120   (  0.000108    0.000104    0.000025 )
   M - matrix:
       0.000038    0.000011    0.000003   (  0.000001    0.000001    0.000000 )
       0.000011    0.000029    0.000001   (  0.000001    0.000001    0.000000 )
       0.000003    0.000001    0.000004   (  0.000000    0.000000    0.000000 )
    unit cell:
       4.42(9)   4.96(5)  12.33(13)       
      90.8(9)  104(1)    108(1)     
      V = 248(6) 
********************** SEARCHING FOR BEST UB STARTED *********************
UM IRUN INFO: Rotation interval: [-2.00,2.00] (deg), number of steps 17 (step: 0.250), indexing rejection criterion: 0.1250
UM IRUN INFO: There are 1 'run' piece flips in the peak table (min=1,max=1)
UB fit with 59 obs out of 916 (total:916,skipped:0) (6.44%)
   UB - matrix:
       0.000896    0.003948   -0.001096   (  0.000037    0.000027    0.000011 )
      -0.002065   -0.003142   -0.001817   (  0.000046    0.000033    0.000014 )
      -0.005910   -0.000145   -0.000156   (  0.000073    0.000053    0.000022 )
   M - matrix:
       0.000038    0.000011    0.000003   (  0.000001    0.000001    0.000000 )
       0.000011    0.000029    0.000001   (  0.000001    0.000001    0.000000 )
       0.000003    0.000001    0.000004   (  0.000000    0.000000    0.000000 )
    unit cell:
       4.42(9)   4.96(5)  12.33(13)       
      90.8(9)  104(1)    108(1)     
      V = 248(6) 
OTKP changes: 58 1 1 1 
Not enough observations available (check whether you can reduce the number of refined pars; currently 8 used reflections and 13 pars)...
OTKP changes: 60 1 1 1 
Not enough observations available (check whether you can reduce the number of refined pars; currently 11 used reflections and 12 pars)...
OTKP changes: 60 1 1 1 
Not enough observations available (check whether you can reduce the number of refined pars; currently 11 used reflections and 11 pars)...
OTKP changes: 60 1 1 1 
OTKP changes: 63 1 1 1 
   UB - matrix:
       0.000738    0.004289   -0.001135   (  0.000028    0.000036    0.000008 )
      -0.001782   -0.003457   -0.001713   (  0.000038    0.000049    0.000011 )
      -0.005683   -0.000247   -0.000029   (  0.000054    0.000070    0.000016 )
   M - matrix:
       0.000036    0.000011    0.000002   (  0.000001    0.000000    0.000000 )
       0.000011    0.000030    0.000001   (  0.000000    0.000000    0.000000 )
       0.000002    0.000001    0.000004   (  0.000000    0.000000    0.000000 )
UB fit with 67 obs out of 916 (total:916,skipped:0) (7.31%)
    unit cell:
       4.49(5)  4.81(3)  12.46(8)       
      91.9(6)  100.0(7)  108.3(8)  
      V = 251(3) 
UB fit with 67 obs out of 916 (total:916,skipped:0) (7.31%)
   UB - matrix:
       0.000738    0.004289   -0.001135   (  0.000028    0.000036    0.000008 )
      -0.001782   -0.003457   -0.001713   (  0.000038    0.000049    0.000011 )
      -0.005683   -0.000247   -0.000029   (  0.000054    0.000070    0.000016 )
   M - matrix:
       0.000036    0.000011    0.000002   (  0.000001    0.000000    0.000000 )
       0.000011    0.000030    0.000001   (  0.000000    0.000000    0.000000 )
       0.000002    0.000001    0.000004   (  0.000000    0.000000    0.000000 )
    unit cell:
       4.49(5)  4.81(3)  12.46(8)       
      91.9(6)  100.0(7)  108.3(8)  
      V = 251(3) 
OTKP changes: 63 1 1 1 
OTKP changes: 65 1 1 1 
   UB - matrix:
       0.000705    0.004186   -0.001107   (  0.000034    0.000044    0.000009 )
      -0.001726   -0.003359   -0.001677   (  0.000044    0.000058    0.000012 )
      -0.005568   -0.000206   -0.000021   (  0.000056    0.000074    0.000016 )
   M - matrix:
       0.000034    0.000010    0.000002   (  0.000001    0.000000    0.000000 )
       0.000010    0.000029    0.000001   (  0.000000    0.000001    0.000000 )
       0.000002    0.000001    0.000004   (  0.000000    0.000000    0.000000 )
UB fit with 70 obs out of 916 (total:916,skipped:0) (7.64%)
    unit cell:
       4.57(5)  4.92(4)  12.73(10)       
      92.1(7)  99.7(8)  107.6(9)   
      V = 268(4) 
916 peaks stored in the peak table
Writing tabbin file: "D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\exp_7302_peakhunt_1"
Run 1 Omega scan: (-63.000 - 61.000,496 frames, 0.250 sec, 0.250 deg) at th=0.000, ka=0.000,ph=0.000 (rot geo dd=663.662)
HKL list info: 1619 refl (0 shortened)
MODEL LIST INFO: Indexation prior to per-frame refinement
UB fit with 70 obs out of 916 (total:916,skipped:0) (7.64%)
    unit cell:
       4.57(5)  4.92(4)  12.73(10)       
      92.1(7)  99.7(8)  107.6(9)   
      V = 268(4) 
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
New UB matrix singular.
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
New UB matrix singular.
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
New UB matrix singular.
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
New UB matrix singular.
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
New UB matrix singular.
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 4 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
New UB matrix singular.
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 1 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 2 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 5 used reflections and 5 pars)...
New UB matrix singular.
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
New UB matrix singular.
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 0 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
New UB matrix singular.
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
Not enough observations available (check whether you can reduce the number of refined pars; currently 3 used reflections and 5 pars)...
PRO INFO: User interrupt from dialog (Thu Sep 19 14:04:55 2024)
User interrupt after cycle 0: isCalibraLSQex in C:\win32\pro\ex94_44_2019_26072023\code\crysalis\util\odxtal\Calibra\calibra5lsqex.cpp
New UB matrix singular.
User interrupt after cycle 0: isCalibraLSQex in C:\win32\pro\ex94_44_2019_26072023\code\crysalis\util\odxtal\Calibra\calibra5lsqex.cpp
New UB matrix singular.
MODEL LIST INFO: Indexation after per-frame refinement
UB fit with 70 obs out of 916 (total:916,skipped:0) (7.64%)

Profile size analysis (per incidence angle)
 Incidence  |         Average profile size - assuming Gaussian shape (in degrees)            |
 angle (deg)|  # of peaks  |   sig_e1 (stddev)   |   sig_e2 (stddev)   |   sig_e3 (stddev)   |
 ---------- | ------------ | ------------------- | ------------------- | ------------------- |
    0- 0.4  |         3    |    0.038 ( 0.005)   |    0.037 ( 0.001)   |    2.199 ( 0.669)   |
  0.4- 0.5  |         3    |    0.046 ( 0.008)   |    0.053 ( 0.024)   |    2.122 ( 0.590)   |
  0.5- 0.5  |         3    |    0.041 ( 0.002)   |    0.041 ( 0.004)   |    1.719 ( 0.410)   |
  0.6- 0.6  |         3    |    0.059 ( 0.044)   |    0.062 ( 0.043)   |    1.605 ( 0.241)   |
  0.6- 0.7  |         3    |    0.040 ( 0.005)   |    0.039 ( 0.007)   |    1.217 ( 0.292)   |
  0.7- 0.7  |         3    |    0.051 ( 0.014)   |    0.037 ( 0.001)   |    2.418 ( 1.311)   |
  0.8- 0.9  |         3    |    0.062 ( 0.035)   |    0.060 ( 0.033)   |    0.721 ( 0.410)   |
  0.9- 0.9  |         3    |    0.033 ( 0.002)   |    0.039 ( 0.001)   |    0.771 ( 0.222)   |
  1.0- 1.2  |         3    |    0.045 ( 0.011)   |    0.028 ( 0.012)   |    0.829 ( 0.261)   |
  1.2- 1.3  |         4    |    0.078 ( 0.056)   |    0.043 ( 0.020)   |    1.529 ( 0.955)   |
 ---------- | ------------ | ------------------- | ------------------- | ------------------- |
    0- 1.3  |        31    |    0.050 ( 0.031)   |    0.044 ( 0.023)   |    1.513 ( 0.867)   |

Fitted profile normalization line parameters
 e1 dimension: a=0.4773 b=0.63
 e2 dimension: a=-0.2271 b=1.17
 e3 dimension: a=-0.7309 b=1.50

Writing tabbin file: "D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_peakhunt"
Writing tabbin file: "D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_proffitpeak"
PROFFITPEAK - Finished at Thu Sep 19 14:04:55 2024
PROFFITMAIN - Started at Thu Sep 19 14:04:55 2024
PROFFITIO INFO: Removing PROFFIT lock file D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302.proffitlock
WD P/CAL INFO: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_cracker.par written
 
Instrument model: dd: 647.00, x0: 388.23, y0: 193.39, beam: 0.00, o0: 0.00, t0: 0.00, k0: 0.00
 
