DC S command at Thu Sep 19 13:59:40 2024 (44.70a 64-bit (release 10-09-2024),compiled Sep 10 2024,13:29:22)
MGC: Program version 0
Experiment: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302
DC INFO: Current KM4 collision model (HyPix3000-100Hz (microED setup), rail: Standard)
System uptime: 1w 3d 2h 12m 25s
EXPECTED FINISH TIME:  (0,496,end:Thu Sep 19 14:01:53 2024)
MEMORY INFO: Image pool: CCD 78.7/276.0 (#69, page size: 4096)

MEMORY INFO: Image pool (microedminimap): CCD 0.0/20.0 (#0, page size: 4096)

Going to -63.000000
GONIO INFO: Goto angle JEOL STAGE with inconsistent angles
Is:-62.9671 (-629671) 
Should:-63.0000 (-630000) 
For further information on messages from the goniometer see: file:__#HELP_EReferenceSection_Issues_ITS_051.html
Run 1 started at Thu Sep 19 13:59:42 2024
Experiment: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302
MicroED Tilt X scan:  -63.000 to   61.000 (  496 frames,   0.250s,   0.250deg) at X: 199.345,Y:-151.314,Z:-158.392,dd: 647.000
DC3 INFO: Shutterless run acquisition (run:1,start frame:1)
CAMHYPIX INFO: overflow threshold = 258122 (max cps = 1048000)
PRO INFO: MicroED/3DED - Stage interrupt from dialog (Thu Sep 19 14:00:12 2024)
ODBENCH Jeol_MicroED INFO:  Device movement interrupted
MicroED Device: Stage scan move with 0.0000 deg additional movement
CAMERA: toggle problem
 - userinterrupt
User interrupt (gim)
CAMHYPIX: user interrupt!
DC3 INFO: waiting for end of 2nd write shutter-less thread...
CAMHYPIX: user interrupt!
DC3 INFO: Shutterless ended with EEXECUTESHUTTERLESSRUN_RETURN_TOGGLE_ at Thu Sep 19 14:00:13 2024 (run:1, frame:116)
Shutterless run 1 ended at Thu Sep 19 14:00:13 2024 with less frames than required due to user interrupt (required=496, done=115)

Run 1 ended at Thu Sep 19 14:00:13 2024

MICROED_MICDEV DEVICE INFO: Shutting down JEOL log ...
DC3 INFO: Waiting for end of data reduction...

Process information (Thu Sep 19 14:00:14 2024)
ID: 16048; threads 59; handles 1549; mem 599896.00 (5968216.00)kB; time: 3d 2h 4m 18s

MEMORY INFO: Memory PF:12345.0, Ph:7183.0, V:5828.0; pDataCollectionHParentDistConcurrentDC3 25
MEMORY INFO: Process info - Handles: 1548, Memory: PF:585.8,peak PF: 966.5, WS: 208.1, peak WS: 533.1
MEMORY INFO: CCD G:6.3,H:159.4 (#1206),V:11.2 (#24)
MEMORY INFO: Tracker: CCD 8.8 (#4)
MEMORY INFO: Image pool: CCD 75.3/276.0 (#66, page size: 4096)
MEMORY INFO: tracker memory not in use!
MEMORY INFO: Image pool (microedminimap): CCD 0.0/20.0 (#0, page size: 4096)
MEMORY INFO: tracker memory not in use!
 
MICROED/3DED INFO: Digest generator ver3 with buffer
MICROEDUTIL_CAP: MicroED license key expires in 2841 days (Wed Jun 30 14:00:14 2032)!
MICROED/3DED INFO: Data set successfully validated for the use with microED-frames-digest (Thu Sep 19 14:00:14 2024)
DC3 INFO: Copy log after experiment not active in Synergy-ED
DC3 INFO: Zip after experiment not active (user-interrupt)
DC3 INFO: Auto cryo shutdown not active (user-interrupt)
! CAMERA ERROR: User interrupt (toggle)
MicroED/3DED - Info:"User requested Queue break during experiment"
MicroED/3DED - Info:"Queue was interrupted during Standard Experiment procedures."
? MicroED/3DED - Error:"Could not finish experiment."
? [Thu Sep 19 14:00:14 2024 ] - MicroED/3DED - Error:"Could not finish Data Collection." - Measurement incomplete (only 115 frames out of 496 collected) 
****************************** MicroED/3DED - single experiment Finished ******************************

Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA Open...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=5...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
Instrument: SynergyED IL1 internal relaxation procedure with high/low set values [D644/0000] and 500 ms wait time.
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E6E2/98C2] and 300 ms wait time.
MicroED/3DED Visual preset: Illumination: Condenser strength 5, Low Condenser range, CL3 Illumination defocus  33% (0xBFD2), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA Open
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
MicroED/3DED IFS Individual Overlay preset (Standard): diff 50CM with FLC OFF, CL3 Illumination defocus multiplier 1.00 (RAW 0xBFD2), exposure time multiplier 1.00
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
MicroED/3DED IFS Individual Overlay preset (Standard): diff 50CM with FLC OFF, CL3 Illumination defocus multiplier 1.00 (RAW 0xBFD2), exposure time multiplier 1.00
XX SCROLL
PRO INFO: Start 'Visual Mode' (Thu Sep 19 14:00:42 2024)
Starting continuous image stream with (visual    0.250s, diff    0.500s) frame time. Using    0.250s
CAMHYPIX: Starting reinit
Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA Open...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=5...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
HYPIX: Shutdown complete!
MicroED/3DED Visual preset: Illumination: Condenser strength 5, Low Condenser range, CL3 Illumination defocus  33% (0xBFD2), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA Open
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
MicroED/3DED IFS Individual Overlay preset (Standard): diff 50CM with FLC OFF, CL3 Illumination defocus multiplier 1.00 (RAW 0xBFD2), exposure time multiplier 1.00
JEOL MICROED CONTROL : Starting internal continuous movement controls thread...
HYPIXDAEMON INFO: Failed to establish connection with the daemon at 192.168.126.70!
CAMHYPIX: HyPix daemon will not be used (iInitInterfaceCAMHYPIX)
Connected to HYPIX system interface (tcpip address: 192.168.126.70 port: 60002,'HyPix cmd')
ServerPhase software version 6.1.0.35
HYPIX INFO: GetDetectorConfig!
 - Number of modules: 1
 - Module #1 ID: 42a7355b0000007e
HYPIX INFO: CalibrationTableList!
 - Cu:6.0keV:8.0keV:10.0keV
Note: In standard modes (16-bit zero dead-time and 31-bit) only single (lower) energy threshold is active!
      Upper threshold is used in dual threshold (differential) mode only.
HYPIX INFO: GetEnv!
 - Temperature at module 1: 37.0
 - Delta T to trim table 1: 6.0
 - Humidity 26.0
 - FG temperature 71.0
CAMHYPIX: MicroED uses Cu table of HyPix
HYPIX INFO: HyPix image folder: 'R:\HyPix-3000' (assumed with full access)

HYPIX CAMERA INTERFACE READY

Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA 50um...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=1...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=C01A...
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E72A/990A] and 300 ms wait time.
MicroED/3DED Preview preset: Illumination: Condenser strength 1, Low Condenser range, CL3 Illumination defocus  33% (0xC01A), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA 50um
Instrument: SynergyED Applying Apt MoveFine (X neg direction, Coarse, 3 times)...
Instrument: SynergyED Applying Apt MoveFine (X neg direction, Coarse, 3 times)...
Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA Open...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=5...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E6E2/98C2] and 300 ms wait time.
MicroED/3DED Visual preset: Illumination: Condenser strength 5, Low Condenser range, CL3 Illumination defocus  33% (0xBFD2), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA Open
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
MicroED/3DED IFS Individual Overlay preset (Standard): diff 50CM with FLC OFF, CL3 Illumination defocus multiplier 1.00 (RAW 0xBFD2), exposure time multiplier 1.00
Opening MicroED Options
Closing MicroED Options
The following changes are applied to 'MicroED options':
MicroED/3DED - Current/Default diffraction optics preset has changed.
MicroED/3DED Preset summary (650 mm Standard) (DD: 647.0 mm): Illumination: Condenser strength 1, Low Condenser range, CL3 Illumination defocus  33% (0xC01A), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x52AF (21167), PLA X: 505 (raw 0x81F8), PLA Y: -115 (raw 0x7F8C), SA 100um
MicroED/3DED - memory for diffraction optics preset ID: 0 has changed.
Diff presets: SA 50um -> SA 100um
MicroED/3DED - Switch current diffraction optics default
MicroED/3DED Diffraction preset (650 mm Standard): Illumination: Condenser strength 1, Low Condenser range, CL3 Illumination defocus  33% (0xC01A), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x52AF (21167), PLA X: 505 (raw 0x81F8), PLA Y: -115 (raw 0x7F8C), SA 100um
DETECTOR DISTANCE (MM):  647.00000 ->   647.00000
Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA 100um...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=1...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=C01A...
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E72A/990A] and 300 ms wait time.
MicroED/3DED Preview preset: Illumination: Condenser strength 1, Low Condenser range, CL3 Illumination defocus  33% (0xC01A), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA 100um
Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA Open...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=5...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E6E2/98C2] and 300 ms wait time.
MicroED/3DED Visual preset: Illumination: Condenser strength 5, Low Condenser range, CL3 Illumination defocus  33% (0xBFD2), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA Open
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
MicroED/3DED IFS Individual Overlay preset (Standard): diff 50CM with FLC OFF, CL3 Illumination defocus multiplier 1.00 (RAW 0xBFD2), exposure time multiplier 1.00
JEOL MICROED CONTROL : Stopping internal continuous movement controls thread...
JEOL MICROED CONTROL : Thread stopped successfully
JEOL MICROED CONTROL : Saving last variables into .ini file.
MicroED/3DED - Stopping the continuous stream.
DC DIFFRACTIONMODESCAN dialog
DC MICROED ACTION: Call MicroED/3DED DC Dialog (Init)
DC MICROED ACTION: Init MicroED/3DED DC dialog
DC MICROED ACTION: New experiment name: exp_7303
DC MICROED ACTION: New grid name: MIL-53-75NH225CH3
Formula Edit Menu: Failed to add menu item info: Import formula from res file
DC MICROED ACTION: End init MicroED/3DED DC dialog
DC MICROED ACTION: New experiment name: exp_730
DC MICROED ACTION: New experiment name: exp_7302
DC MICROED ACTION: Button CLEAR PATH was pressed
DELETE INFO (RECYCLING BIN): Deleting files in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\e*.*)
DELETE INFO (RECYCLING BIN): Deleting files in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\*.geo)
DELETE INFO (RECYCLING BIN): Deleting files in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\*.ccd)
DELETE INFO (RECYCLING BIN): Deleting files in tmp directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\tmp\*.*)
DELETE INFO (RECYCLING BIN): Deleting files in frames directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\frames\*.*)
DELETE INFO (RECYCLING BIN): Deleting files in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\pre_*.*)
DELETE INFO: Deleting files in log directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\log\*.txt)
DELETE INFO (RECYCLING BIN): Deleting files in dc plots directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_dc\*.dat)
DELETE INFO (RECYCLING BIN): Deleting files in exp info directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\expinfo\*.ini)
DELETE INFO (RECYCLING BIN): Deleting files in red plots directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\plots_red\*.dat)
DELETE INFO (RECYCLING BIN): Deleting run file in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302.run)
DELETE INFO (RECYCLING BIN): Deleting par file in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302.par)
DELETE INFO (RECYCLING BIN): Deleting sum file in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\*.sum)
DELETE INFO (RECYCLING BIN): Deleting bup file in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\*.bup)
DELETE INFO (RECYCLING BIN): Deleting bup file in bup subdirectory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\bup\*.bup)
DELETE INFO (RECYCLING BIN): Deleting flood file in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\*.ff*)
DELETE INFO (RECYCLING BIN): Deleting files in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\scr_*.*)
DELETE INFO (RECYCLING BIN): Deleting bup file in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\*.runbup)
DELETE INFO (RECYCLING BIN): Deleting bup file in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\*.hklauto)
DELETE INFO (RECYCLING BIN): Deleting bup file in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\*.tabbin)
DELETE INFO (RECYCLING BIN): Deleting ini files in root directory... (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\*.ini)
DC MICROED ACTION: formula
DC MICROED ACTION: Al C H N O
DC MICROED ACTION: Set current directory to: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302
DC MICROED ACTION: Experiment grid name: MIL-53-75NH225CH3
DC MICROED ACTION: Experiment file name: exp_7302
MICROED/3DED DC INFO: User resolution 0.800 (D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\expinfo\exp_7302_preexp_settings.ini)
DC MICROED ACTION: done ok end
DC MICROED ACTION: START EXPERIMENT button was pressed
DC MICROED ACTION: pcleanupmicroeddc start
DC MICROED ACTION: pcleanupmicroeddc end
DC MICROED ACTION: MicroED/3DED DC Dialog was closed, Return value: 1
DC MICROED ACTION: Start copy snaps...
MICROED/3DED DC INFO: Copying visual snap image to D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_microed_grain_snapshot.jpg- FAILED
MICROED/3DED DC INFO: Copying visual snap image to D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_microed_grain_snapshot.rodhypix- FAILED
MICROED/3DED DC INFO: Copying visual snap image to D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_microed_grain_snapshot.tiff- FAILED
DC MICROED ACTION: End copy snaps...
Saved image path: FILE:D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_microed_minimap_snapshot.tiff
WD MEDMMJPG: Saved minimap jpg image path: D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302\exp_7302_microed_minimap_snapshot_199_-151.jpg
DC MICROED ACTION: Making minimap images done...
DC MICROED ACTION: destroy microeddc structures (iwDestroyMicroEDDCMICROEDDC)
DC MICROED ACTION: pcleandatamicroeddc finally block started
DC MICROED ACTION: pcleandatamicroeddc finally block ended
****************************** MicroED/3DED - Experiment settings summary******************************

****************************** MicroED/3DED - General ******************************

Experiment 'exp_7302' by 'Khai' in 'D:\Khai\Delft\SAN14-2\MIL-53-75NH225CH3\exp_7302'

Experiment Stage position : X: 0.00, Y: 0.00, Z: 0.00

Scan range: -63.00 - 61.00 deg, Exp Time: 1.00 s/deg, scan width 0.25 deg, optics preset: 650 mm Standard.

Estimated exp duration time: 02m 00s .

Estimated exp finish time: Thu Sep 19 14:03:51 2024.

Concurrent data reduction - AutoChem

****************************** MicroED/3DED - Pre operations settings ******************************

Center XY - Image processing reposition/compensation - DISABLED.

Center Z - Image processing height compensation - DISABLED.

Primary beam - PLA centering - ENABLED.

****************************** MicroED/3DED - Post operations settings ******************************

EDS measurement - DISABLED.

Tomography - Real space measurement (Visual Scan) - DISABLED.

Single frame at given tilt position - ENABLED.

Single post experiment image at 0.00 deg with 5.00 s exposure time, IFS optics preset: High-res.

