DC S command at Thu Sep 19 12:55:32 2024 (44.70a 64-bit (release 10-09-2024),compiled Sep 10 2024,13:29:22)
MGC: Program version 0
Experiment: D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7299\exp_7299
DC INFO: Current KM4 collision model (HyPix3000-100Hz (microED setup), rail: Standard)
System uptime: 1w 3d 1h 8m 17s
EXPECTED FINISH TIME:  (0,504,end:Thu Sep 19 12:57:47 2024)
MEMORY INFO: Image pool: CCD 78.7/276.0 (#69, page size: 4096)

MEMORY INFO: Image pool (microedminimap): CCD 0.0/20.0 (#0, page size: 4096)

Going to -63.000000
GONIO INFO: Goto angle JEOL STAGE with inconsistent angles
Is:-63.0176 (-630176) 
Should:-63.0000 (-630000) 
For further information on messages from the goniometer see: file:__#HELP_EReferenceSection_Issues_ITS_051.html
Run 1 started at Thu Sep 19 12:55:34 2024
Experiment: D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7299\exp_7299
MicroED Tilt X scan:  -63.000 to   63.000 (  504 frames,   0.250s,   0.250deg) at X:-113.795,Y: -12.431,Z: -78.785,dd: 647.000
DC3 INFO: Shutterless run acquisition (run:1,start frame:1)
CAMHYPIX INFO: overflow threshold = 258122 (max cps = 1048000)
MicroED Device: Stage scan move with 0.0000 deg additional movement
DC3 INFO: Shutterless ended OK at Thu Sep 19 12:57:44 2024 (run:1, frame:504)
Run 1 ended at Thu Sep 19 12:57:44 2024

Data collection successfully finished at Thu Sep 19 12:57:44 2024
MICROED_MICDEV DEVICE INFO: Shutting down JEOL log ...
DC3 INFO: Waiting for end of data reduction...

Launching CrysAlis program... (1) (Thu Sep 19 12:57:46 2024)
Launch mode: MODE_CURRENTEXP_CONCURRENT

Process information (Thu Sep 19 12:57:47 2024)
ID: 16048; threads 58; handles 1549; mem 752588.00 (6114440.00)kB; time: 3d 1h 1m 51s

MEMORY INFO: Memory PF:12910.0, Ph:7742.0, V:5971.0; pDataCollectionHParentDistConcurrentDC3 25
MEMORY INFO: Process info - Handles: 1548, Memory: PF:734.9,peak PF: 966.5, WS: 355.1, peak WS: 533.1
MEMORY INFO: CCD G:6.3,H:159.4 (#1206),V:11.2 (#24)
MEMORY INFO: Tracker: CCD 8.8 (#4)
MEMORY INFO: Image pool: CCD 75.3/276.0 (#66, page size: 4096)
MEMORY INFO: tracker memory not in use!
MEMORY INFO: Image pool (microedminimap): CCD 0.0/20.0 (#0, page size: 4096)
MEMORY INFO: tracker memory not in use!
 
MICROED/3DED INFO: Digest generator ver3 with buffer
MICROEDUTIL_CAP: MicroED license key expires in 2841 days (Wed Jun 30 12:57:47 2032)!
MICROED/3DED INFO: Data set successfully validated for the use with microED-frames-digest (Thu Sep 19 12:57:47 2024)
DC3 INFO: Copy log after experiment not active in Synergy-ED
DC3 INFO: Zip after experiment not active
DC3 INFO: Auto cryo shutdown not active
Parking goniometer at requested position (Thu Sep 19 12:57:47 2024)...
Going to 0.000000
GONIO INFO: Goto angle JEOL STAGE with inconsistent angles
Is:-0.5430 (-5430) 
Should:0.0000 (0) 
For further information on messages from the goniometer see: file:__#HELP_EReferenceSection_Issues_ITS_051.html
****************************** MicroED/3DED - Single image requested ******************************

MicroED/3DED - Info:"Reconstructing optics preset."
Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA Open...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=5...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
Instrument: SynergyED IL1 internal relaxation procedure with high/low set values [D644/0000] and 500 ms wait time.
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E6E2/98C2] and 300 ms wait time.
MicroED/3DED Visual preset: Illumination: Condenser strength 5, Low Condenser range, CL3 Illumination defocus  33% (0xBFD2), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA Open
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
MicroED/3DED IFS Individual Overlay preset (Standard): diff 50CM with FLC OFF, CL3 Illumination defocus multiplier 1.00 (RAW 0xBFD2), exposure time multiplier 1.00
Instrument: SynergyED Applying mag2 X15K...
Instrument: SynergyED Applying CL3 Illumination defocus=A95C...
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [D06C/824C] and 300 ms wait time.
MicroED/3DED IFS Individual Overlay preset (High-res): mag2 X15K with FLC OFF, CL3 Illumination defocus multiplier 0.30 (RAW 0xA95C), exposure time multiplier 4.00
MicroED/3DED - Info:"Reconstructing Stage tilt position."
MicroED/3DED - Info:"Single image acquisition"
CAMHYPIX INFO: overflow threshold = 5236122 (max cps = 1048000)
MicroED/3DED - Info:"Auto adjusting Look Up Table settings, based on current image. "
LUT adjusted 1307 -> 1309 
MicroED/3DED - Info:"Saving all requested formats - single image"
Image saved to FILE:D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7299\exp_7299_microed_post_snapshot.jpg
Saved image path: FILE:D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7299\exp_7299_microed_post_snapshot.tiff
Single image saved to FILE:D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7299\exp_7299_microed_post_snapshot.rodhypix
MicroED/3DED - Info:"Auto adjusting Look Up Table - settings reverted."
****************************** MicroED/3DED - single experiment Finished ******************************

Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA Open...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=5...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
Instrument: SynergyED IL1 internal relaxation procedure with high/low set values [D644/0000] and 500 ms wait time.
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E6E2/98C2] and 300 ms wait time.
MicroED/3DED Visual preset: Illumination: Condenser strength 5, Low Condenser range, CL3 Illumination defocus  33% (0xBFD2), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA Open
Instrument: SynergyED Applying mag2 X15K...
Instrument: SynergyED Applying CL3 Illumination defocus=A95C...
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [D06C/824C] and 300 ms wait time.
MicroED/3DED IFS Individual Overlay preset (High-res): mag2 X15K with FLC OFF, CL3 Illumination defocus multiplier 0.30 (RAW 0xA95C), exposure time multiplier 4.00
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E6E2/98C2] and 300 ms wait time.
MicroED/3DED IFS Individual Overlay preset (Standard): diff 50CM with FLC OFF, CL3 Illumination defocus multiplier 1.00 (RAW 0xBFD2), exposure time multiplier 1.00
XX SCROLL
PRO INFO: Start 'Visual Mode' (Thu Sep 19 12:59:12 2024)
Starting continuous image stream with (visual    0.250s, diff    0.500s) frame time. Using    0.250s
Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA Open...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=5...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
CAMHYPIX INFO: overflow threshold = 258122 (max cps = 1048000)
MicroED/3DED Visual preset: Illumination: Condenser strength 5, Low Condenser range, CL3 Illumination defocus  33% (0xBFD2), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA Open
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
MicroED/3DED IFS Individual Overlay preset (Standard): diff 50CM with FLC OFF, CL3 Illumination defocus multiplier 1.00 (RAW 0xBFD2), exposure time multiplier 1.00
JEOL MICROED CONTROL : Starting internal continuous movement controls thread...
No difference was found in a requested position compared to the current one, JEOL stage movement skipped
Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA 50um...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=1...
Instrument: SynergyED Applying ILFocus=52AF...
Instrument: SynergyED Applying PLA X/Y = 493 / -99 (raw 0x81EC/0x7F9C) ...
Instrument: SynergyED Applying CL3 Illumination defocus=C01A...
Instrument: SynergyED IL1 internal relaxation procedure with high/low set values [D2AF/0000] and 500 ms wait time.
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E72A/990A] and 300 ms wait time.
MicroED/3DED Diffraction preset (650 mm Standard): Illumination: Condenser strength 1, Low Condenser range, CL3 Illumination defocus  33% (0xC01A), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x52AF (21167), PLA X: 493 (raw 0x81EC), PLA Y: -99 (raw 0x7F9C), SA 50um
MicroED/3DED - Stopping the continuous stream.
MicroED/3DED - Starts continuous stream.
xx stream 0.0
Starting continuous image stream with (visual    0.250s, diff    0.500s) frame time. Using    0.500s
CAMHYPIX INFO: overflow threshold = 520122 (max cps = 1048000)
Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA Open...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=5...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
Instrument: SynergyED IL1 internal relaxation procedure with high/low set values [D644/0000] and 500 ms wait time.
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E6E2/98C2] and 300 ms wait time.
MicroED/3DED Visual preset: Illumination: Condenser strength 5, Low Condenser range, CL3 Illumination defocus  33% (0xBFD2), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA Open
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
MicroED/3DED IFS Individual Overlay preset (Standard): diff 50CM with FLC OFF, CL3 Illumination defocus multiplier 1.00 (RAW 0xBFD2), exposure time multiplier 1.00
MicroED/3DED - Stopping the continuous stream.
MicroED/3DED - Starts continuous stream.
xx stream 0.0
Starting continuous image stream with (visual    0.250s, diff    0.500s) frame time. Using    0.250s
CAMHYPIX INFO: overflow threshold = 258122 (max cps = 1048000)
Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA 50um...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=1...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=C01A...
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E72A/990A] and 300 ms wait time.
MicroED/3DED Preview preset: Illumination: Condenser strength 1, Low Condenser range, CL3 Illumination defocus  33% (0xC01A), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA 50um
Instrument: SynergyED Applying Apt MoveFine (X pos direction, Coarse, 3 times)...
Instrument: SynergyED Applying Apt MoveFine (X pos direction, Coarse, 3 times)...
Instrument: SynergyED Applying Apt MoveFine (X pos direction, Coarse, 3 times)...
Instrument: SynergyED Applying Apt MoveFine (X pos direction, Coarse, 3 times)...
Instrument: SynergyED Applying Apt MoveFine (X pos direction, Coarse, 3 times)...
Instrument: SynergyED Applying Apt MoveFine (X pos direction, Coarse, 3 times)...
Instrument: SynergyED Applying Apt MoveFine (Y pos direction, Coarse, 3 times)...
Instrument: SynergyED Applying Apt MoveFine (X pos direction, Coarse, 3 times)...
Instrument: SynergyED Applying Condenser range=Low...
Instrument: SynergyED Applying CL 30um...
Instrument: SynergyED Applying SA Open...
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying SpotSize=5...
Instrument: SynergyED Applying ILFocus=5644...
Instrument: SynergyED Applying PLA X/Y = 645 / 5 (raw 0x8284/0x8004) ...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
Instrument: SynergyED CL3 internal relaxation procedure with high/low set values [E6E2/98C2] and 300 ms wait time.
MicroED/3DED Visual preset: Illumination: Condenser strength 5, Low Condenser range, CL3 Illumination defocus  33% (0xBFD2), CL 30um
Projection: Magnification diff 50CM, IL1 Projection focus: 0x5644 (22084), PLA X: 645 (raw 0x8284), PLA Y: 5 (raw 0x8004), SA Open
Instrument: SynergyED Applying diff 50CM...
Instrument: SynergyED Applying CL3 Illumination defocus=BFD2...
MicroED/3DED IFS Individual Overlay preset (Standard): diff 50CM with FLC OFF, CL3 Illumination defocus multiplier 1.00 (RAW 0xBFD2), exposure time multiplier 1.00
JEOL MICROED CONTROL : Stopping internal continuous movement controls thread...
JEOL MICROED CONTROL : Thread stopped successfully
JEOL MICROED CONTROL : Saving last variables into .ini file.
MicroED/3DED - Stopping the continuous stream.
DC DIFFRACTIONMODESCAN dialog
DC MICROED ACTION: Call MicroED/3DED DC Dialog (Init)
DC MICROED ACTION: Init MicroED/3DED DC dialog
DC MICROED ACTION: New experiment name: exp_7300
DC MICROED ACTION: New grid name: MIL-53-5NH295CH3
Formula Edit Menu: Failed to add menu item info: Import formula from res file
DC MICROED ACTION: End init MicroED/3DED DC dialog
DC MICROED ACTION: formula
DC MICROED ACTION: Al C H N O
DC MICROED ACTION: Set current directory to: D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7300
DC MICROED ACTION: Experiment grid name: MIL-53-5NH295CH3
DC MICROED ACTION: Experiment file name: exp_7300
MICROED/3DED DC INFO: User resolution 0.800 (D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7300\expinfo\exp_7300_preexp_settings.ini)
DC MICROED ACTION: done ok end
DC MICROED ACTION: START EXPERIMENT button was pressed
DC MICROED ACTION: pcleanupmicroeddc start
DC MICROED ACTION: pcleanupmicroeddc end
DC MICROED ACTION: MicroED/3DED DC Dialog was closed, Return value: 1
DC MICROED ACTION: Start copy snaps...
MICROED/3DED DC INFO: Copying visual snap image to D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7300\exp_7300_microed_grain_snapshot.jpg- FAILED
MICROED/3DED DC INFO: Copying visual snap image to D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7300\exp_7300_microed_grain_snapshot.rodhypix- FAILED
MICROED/3DED DC INFO: Copying visual snap image to D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7300\exp_7300_microed_grain_snapshot.tiff- FAILED
DC MICROED ACTION: End copy snaps...
Saved image path: FILE:D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7300\exp_7300_microed_minimap_snapshot.tiff
WD MEDMMJPG: Saved minimap jpg image path: D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7300\exp_7300_microed_minimap_snapshot_127_-112.jpg
DC MICROED ACTION: Making minimap images done...
DC MICROED ACTION: destroy microeddc structures (iwDestroyMicroEDDCMICROEDDC)
DC MICROED ACTION: pcleandatamicroeddc finally block started
DC MICROED ACTION: pcleandatamicroeddc finally block ended
****************************** MicroED/3DED - Experiment settings summary******************************

****************************** MicroED/3DED - General ******************************

Experiment 'exp_7300' by 'Khai' in 'D:\Khai\Delft\SAN14-2\MIL-53-5NH295CH3\exp_7300'

Experiment Stage position : X: 0.00, Y: 0.00, Z: 0.00

Scan range: -63.00 - 62.00 deg, Exp Time: 1.00 s/deg, scan width 0.25 deg, optics preset: 650 mm Standard.

Estimated exp duration time: 02m 00s .

Estimated exp finish time: Thu Sep 19 13:04:20 2024.

Concurrent data reduction - AutoChem

****************************** MicroED/3DED - Pre operations settings ******************************

Center XY - Image processing reposition/compensation - DISABLED.

Center Z - Image processing height compensation - DISABLED.

Primary beam - PLA centering - ENABLED.

****************************** MicroED/3DED - Post operations settings ******************************

EDS measurement - DISABLED.

Tomography - Real space measurement (Visual Scan) - DISABLED.

Single frame at given tilt position - ENABLED.

Single post experiment image at 0.00 deg with 5.00 s exposure time, IFS optics preset: High-res.

